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| United States Patent Application |
20080297808
|
| Kind Code
|
A1
|
|
Riza; Nabeel Agha
;   et al.
|
December 4, 2008
|
Optical Sensor For Extreme Environments
Abstract
An optical sensing probe includes a tube having a tip portion configured
for placement in an environment in which conditions are to be sensed and
an etalon having a known characteristic disposed proximate the tip
portion. The tube also includes a head portion remote from the tip
portion containing a light directing element for directing light beams at
the etalon and receiving reflected light beams from the etalon wherein
the received reflected light beams are used for determining an
environmental condition proximate the tip portion. A method for measuring
a thickness of the etalon may include directing a light beams at
different frequencies at the etalon and receiving the light beams from
the etalon. The method may also include identifying conditions of the
respective light beams condition received from the etalon and then
calculating a first thickness of the etalon responsive to the respective
conditions and the known characteristic.
| Inventors: |
Riza; Nabeel Agha; (Oviedo, FL)
; Perez; Frank; (Tujunga, CA)
|
| Correspondence Address:
|
BEUSSE WOLTER SANKS MORA & MAIRE, P. A.
390 NORTH ORANGE AVENUE, SUITE 2500
ORLANDO
FL
32801
US
|
| Serial No.:
|
567600 |
| Series Code:
|
11
|
| Filed:
|
December 6, 2006 |
| Current U.S. Class: |
356/503; 356/630 |
| Class at Publication: |
356/503; 356/630 |
| International Class: |
G01B 11/28 20060101 G01B011/28; G01B 11/02 20060101 G01B011/02 |
Claims
1. A method for measuring a thickness of an etalon comprising:directing a
first light beam at a first frequency and a second light beam at a second
frequency at a first portion of an etalon having a known
characteristic;receiving the first light beam and the second light beam
from the etalon; andidentifying a first condition of the first light beam
and a second condition of the second light beam received from the etalon;
andcalculating a first thickness of the etalon responsive to the first
condition, the second condition, and the known characteristic.
2. The method of claim 1, wherein the first condition comprises at least
one of an interference maximum and an interference minimum of the first
light beam.
3. The method of claim 2, wherein the second condition comprises at least
one of an interference maximum and an interference minimum of the second
light beam.
4. The method of claim 3, further comprising determining respective
refractive indices of the etalon for the at least one of the interference
maximum and the interference minimum of the first light beam and for the
at least one of the interference maximum and the interference minimum of
the second light beam.
5. The method of claim 4, wherein the respective refractive indices are
determined according to a Sellmeier equation.
6. The method of claim 4, wherein the first thickness is calculated
according to the
formula:t=(.lamda.1*.lamda.2)/(2*(.lamda.2*n1-.lamda.1*n2));where t is
the first thickness; .lamda.1 is a wavelength of the first frequency,
.lamda.2 is a wavelength of the second frequency, n1 is the refractive
index at the first frequency, and n2 is the refractive index at the
second frequency.
7. The method of claim 3, wherein the first condition and second condition
correspond to adjacent at least one of the interference maximum and
minimum of the first light beam and at least one of the interference
maximum and minimum of the second light beam.
8. The method of claim 7, further comprising:calculating at least a second
thickness for a different first frequency and a different second
frequency; andcalculating an average thickness corresponding to at least
the first thickness and the second thicknesses.
9. The method of claim 1, further comprising:moving the etalon relative to
the first light beam and the second light beam to align the beams with a
second portion of the etalon;performing the steps of claim 1 to calculate
the thickness of a second portion of the etalon.
10. The method of claim 1, further comprising:disposing the etalon in an
environment in which conditions are to be sensed; andusing the calculated
thickness to determine an environmental condition proximate the etalon.
11. The method of claim 10, wherein the environmental conditions comprise
at least one of a temperature and a pressure.
12. The method of claim 1, wherein the light beams are directed to impinge
upon a surface of the etalon at an angle normal to the surface.
13. The method of claim 1, wherein the known characteristic comprises a
relationship between a refractive index of the etalon and wavelength of
light incident on the etalon.
14. The method of claim 13, wherein the relationship comprises a Sellmeier
equation for the etalon.
15. The method of claim 1, wherein the etalon comprises silicon carbide.
16. The method of claim 1, wherein the etalon comprises a single crystal
silicon carbide.
17. A system for measuring a thickness of an etalon comprising:a first
light source for directing a first light beam having a first wavelength
at a first portion of an etalon having a known characteristic;a second
light source for directing a second light beam having a second wavelength
different from the first wavelength at the etalon;an optical receiver for
receiving the first light beam and the second light beam from the etalon
and for providing a first power signal corresponding to the first light
beam received from the etalon and a second power signal corresponding to
the second light beam received from the etalon; anda processor for
identifying a first condition of the first power signal and a second
condition of the second power signal received from optical receiver and
calculating a thickness of the etalon responsive to the first condition,
the second condition, and the known characteristic.
18. The system of claim 17, wherein the first light beam and the second
light beam are directed to impinge upon a surface of the etalon at an
angle normal to the surface.
19. The system of claim 17, wherein the first light source and the second
light source comprise a single laser capable of selectively generating
light at the first wavelength and the second wavelength.
20. The system of claim 17, wherein the first light source and the second
light source comprise a single broadband light source.
21. The system of claim 17, wherein the light beams are directed at the
etalon along a light path comprising at least a free space portion.
22. The system of claim 21, wherein the light path comprises a single mode
optical fiber and a collimator.
23. The system of claim 22, wherein the collimator comprises at least one
of a fiber collimating self imaging lens and a fiber imaging lens
24. The system of claim 21, wherein the etalon is disposed at a minimum
light beam waist location in the free space portion.
25. The system of claim 21, further comprising a polarizer disposed in the
light path in the free space portion.
26. The system of claim 17, further comprising a circulator for separating
the light beams directed at the etalon from the light beams received from
the etalon.
27. The system of claim 22, wherein the single mode fiber is configured to
function as a pin hole for allowing optimization of a light beam
incidence angle on the etalon.
28. The system of claim 17, wherein the optical receiver comprises at
least one of an optical detector and an optical spectrum analyzer.
29. An optical sensing probe comprising a tube having a tip portion
configured for placement in an environment in which conditions are to be
sensed, an etalon having a known characteristic that changes responsive
to an environmental condition disposed proximate the tip portion; and a
head portion remote from the tip portion containing a light directing
element for directing light beams at the etalon and receiving reflected
light beams from the etalon wherein the received reflected light beams
are used for determining an environmental condition proximate the tip
portion.
30. The probe of claim 29, further comprising a fiber bundle for
conducting respective portions of the light beams between the head
portion and the etalon.
31. The probe of claim 29, further comprising a light source for providing
a first light beam at a first frequency and a second light beam at a
second frequency to the light directing element.
32. The probe of claim 29, further comprising a processor for identifying
a first condition of the first light beam reflected from the etalon and a
second condition of the first light beam reflected from the etalon and
calculating a thickness of the etalon responsive to the first condition,
the second condition, and the known characteristic.
33. The probe of claim 29, wherein the etalon is configured to seal an
interior of the tube proximate the tip.
34. The probe of claim 33, further comprising a window configured to seal
an interior the tube proximate the head.
35. The probe of claim 34, wherein the interior of the tube contains at
least a partial vacuum.
36. The probe of claim 29, further comprising a tip cage disposed around
the tip portion proximate the etalon for providing protection of the
etalon.
38. The probe of claim 29, wherein the etalon comprises single crystal
silicon carbide.
40. The probe of claim 29, wherein the tip portion comprises a material
having a coefficient of thermal expansion about the same as the etalon
effective to limit heat induced stresses on the etalon.
42. The probe of claim 29, wherein at least a portion of the tube
comprises a material having a lower coefficient of thermal conductivity
than the tip portion.
43. The probe of claim 29, further comprising at least one telescoping
portion between the head portion and the tip portion.
44. The probe of claim 29, wherein the light directing element further
comprises a mechanism for aiming the light beams at the etalon to achieve
a desired light incidence angle with respect to a surface of the etalon.
45. The probe of claim 29, wherein the light directing element further
comprises a polarizer disposed in a light beam path of the light beams.
46. The probe of claim 29, wherein the tip portion and the head portion
comprise two separate elements configured for allowing passage of the
light beams therethrough.
47. The probe of claim 29, wherein a plurality of tubes are disposed
within a tip housing around a least the respective tip portions of the
tubes.
48. The probe of claim 47, wherein the respective head portions
corresponding to the plurality of tubes comprise separate elements
disposed within a head housing around the respective head portions of the
tubes.
49. The probe of claim 29, wherein the etalon is attached to a rotating
element and the tube is disposed relative to the rotating element for
directing the light beams at the etalon and receiving the reflected light
beams from the etalon when the etalon is positioned within a light path
of the light beams as the rotating element moves the etalon into the
light path.
50. The probe of claim 49, wherein the rotating element comprises at least
one of a wheel and a turbine blade.
51. The probe of claim 50, wherein the tube is disposed proximate a
support structure of the wheel.
52. The probe of claim 49, further comprising a support element for
attaching the etalon to the rotating element.
53. The probe of claim 52, wherein the support element comprises a
material having a coefficient of thermal expansion about the same as the
etalon for limiting heat induced stresses on the etalon.
54. The probe of claim 52, wherein the support element comprises a
material having a lower coefficient of thermal conductivity than the
etalon.
55. The probe of claim 29, wherein the etalon is configured to deform
responsive to a pressure differential on opposite surfaces of the etalon
sufficiently for being sensed by the probe as a received light beam cross
section difference from a transmitted light beam cross section.
56. The probe of claim 55, further comprising at least one beam expansion
lens disposed in a light path of the light beams for increasing the
transmitted light beam cross section for impinging on a relatively larger
surface of the etalon.
57. The probe of claim 29, further comprising a two dimensional optical
detector for generating an image responsive to the received beams.
58. The probe of claim 57, further comprising an image processor in
communication with the two dimensional optical detector for analyzing at
least a portion of the image to determine a temperature of the etalon.
59. The probe of claim 57, further comprising an image processor in
communication with the two dimensional optical detector for analyzing the
image to determine at least one of a pressure and a pressure distribution
on the etalon.
60. The probe of claim 57, further comprising a beam splitter disposed in
a light path of the light beams for directing the received light beams to
the two dimensional optical detector.
61. The probe of claim 29, further comprising a point detector for
receiving at least a portion of the received light beams for indicating
an alignment condition of the light beams with respect to the etalon.
62. An optical sensor comprising:a chamber having an inlet for receiving a
fluid into the chamber, an aperture formed in a wall of the chamber, and
an etalon having a known characteristic that changes responsive to an
environmental condition sealing the aperture; anda light directing
element for directing light beams at the etalon and receiving reflected
light beams from the etalon, wherein the reflected light beams are used
for determining an environmental condition in the chamber.
63. The sensor of claim 62, further comprising a light source for
providing a first light beam at a first frequency and a second light beam
at a second frequency to the light directing element.
64. The sensor of claim 62, further comprising a processor for identifying
a first condition of the first light beam reflected from the etalon and a
second condition of the first light beam reflected from the etalon and
calculating a thickness of the etalon responsive to the first condition,
the second condition, and the known characteristic.
65. The sensor of claim 62, further comprising a two dimensional optical
detector for generating an image responsive to the received light beams.
66. The sensor of claim 65, further comprising an image processor in
communication with the two dimensional optical detector for analyzing the
image to determine a pressure on the etalon.
67. The sensor of claim 62, wherein the light directing element comprises
a single mode fiber for emitting the light beams along a free space path
to the etalon and receiving the reflected light beams from the free space
path.
68. The sensor of claim 67, further comprising a lens for focusing the
emitted light beams and received light beams on a focused spot of the
etalon.
69. The sensor of claim 67, further comprising a lens for collimating the
emitted light beams and received light beams on majority portion of the
surface of the etalon.
70. The sensor of claim 62, wherein the light directing element further
comprises a mechanism for aiming the light beams at the etalon to achieve
a desired light incidence angle with respect to a surface of the etalon.
71. The sensor of claim 70, wherein the mechanism comprises a tilt
element.
72. The sensor of claim 70, wherein the mechanism comprises a translation
element.
Description
SPECIFIC DATA RELATED TO INVENTION
[0001]This application claims the benefit of U.S. provisional application
No. 60/742,813 filed on Dec. 6, 2005.
BACKGROUND OF INVENTION
[0002]The present invention relates to optical sensors and, more
particularly, to optical sensors using etalons for remote sensing in
extreme environments.
[0003]There are numerous vital sensing scenarios in commercial and defense
sectors where the environment is extremely hazardous. Specifically, the
hazards can be for instance due to extreme temperatures, extreme
pressures, highly corrosive chemical content (liquids, gases,
particulates), nuclear radiation, biological agents, and high
Gravitational (G) forces. Realizing a sensor for such hazardous
environments remains to be a tremendous engineering challenge. One
specific application is fossil fuel fired power plants where temperatures
in combustors and turbines typically have temperatures and pressures
exceeding 1000.degree. C. and 50 Atmospheres (atm). Future clean design
zero emission power systems are expected to operate at even high
temperatures and pressures, e.g., >2000.degree. C. and >400 atm [J.
H. Ausubel, "Big Green Energy Machines," The Industrial Physicist, AIP,
pp. 20-24, October/November, 2004.] In addition, coal and gas fired power
systems produce chemically hazardous environments with chemical
constituents and mixtures containing for example carbon monoxide, carbon
dioxide, nitrogen, oxygen, sulphur, sodium, and sulphuric acid. Over the
years, engineers have worked very hard in developing electrical high
temperature sensors (e.g., thermo-couples using platinum and rodium), but
these have shown limited life-times due to the wear and tear and
corrosion suffered in power plants [R. E. Bentley, "Thermocouple
materials and their properties," Chap. 2 in Theory and Practice of
Thermoelectric Thermometry: Handbook of Temperature Measurement, Vol. 3,
pp. 25-81, Springer-Verlag Singapore, 1998].
[0004]Researchers have turned to optics for providing a robust high
temperature sensing solution in these hazardous environments. The focus
of these researchers have been mainly directed in two themes. The first
theme involves using the optical fiber as the light delivery and
reception mechanism and the temperature sensing mechanism. Specifically,
a Fiber Bragg Grating (FBG) present within the core of the single mode
fiber (SMF) acts as a temperature sensor. Here, a broadband light source
is fed to the sensor and the spectral shift of the FBG reflected light is
used to determine the temperature value. Today, commercial FBG sensors
are written using Ultra-Violet (UV) exposure in silica fibers. Such FBG
sensors are typically limited to under 600.degree. C. because of the
instability of the FBG structure at higher temperatures [B. Lee, "Review
of the present status of optical fiber sensors," Optical Fiber
Technology, Vol. 9, pp. 57-79, 2003]. Recent studies using FBGs in silica
fibers has shown promise up-to 1000.degree. C. [M. Winz, K. Stump, T. K.
Plant, "High temperature stable fiber Bragg gratings, "Optical Fiber
Sensors (OFS) Conf. Digest, pp. 195 198, 2002; D. Grobnic, C. W. Smelser,
S. J. Mihailov, R. B. Walker," Isothermal behavior of fiber Bragg
gratings made with ultrafast radiation at temperatures above 1000 C,"
European Conf. Optical Communications (ECOC), Proc. Vol. 2, pp. 130-131,
Stockholm, Sep. 7, 2004]. To practically reach the higher temperatures
(e.g., 1600.degree. C.) for fossil fuel applications, single crystal
Sapphire fiber has been used for Fabry-Perot cavity and FBG formation [H.
Xiao, W. Zhao, R. Lockhart, J. Wang, A. Wang, "Absolute Sapphire optical
fiber sensor for high temperature applications," SPIE Proc. Vol. 3201,
pp. 36-42, 1998; D. Grobnic, S. J. Mihailov, C. W. Smelser, H. Ding,
"Ultra high temperature FBG sensor made in Sapphire fiber using
Isothermal using femtosecond laser radiation," European Conf. Optical
Communications (ECOC), Proc. Vol. 2, pp. 128-129, Stockholm, Sep. 7,
2004]. The single crystal Sapphire fiber FBG has a very large diameter
(e.g., 150 microns) that introduces multi-mode light propagation noise
that limits sensor performance. An alternate approach [see Y. Zhang, G.
R. Pickrell, B. Qi, A. S. -Jazi, A. Wang, "Single-crystal sapphire-based
optical high temperature sensor for harsh environments," Opt. Eng., 43,
157-164, 2004] described replaced the Sapphire fiber frontend sensing
element with a complex assembly of individual components that include a
Sapphire bulk crystal that forms a temperature dependent birefringent
Fabry-Perot cavity, a single crystal cubic zirconia light reflecting
prism, a Glan-Thompson polarizer, a single crystal Sapphire assembly
tube, a fiber collimation lens, a ceramic extension tube, and seven 200
micron diameter multimode optical fibers. Hence this described sensor
frontend sensing element not only has low optical efficiency and high
noise generation issues due to its multi-mode versus SMF design, the
sensor frontend is limited by the lowest high temperature performance of
a given component in the assembly and not just by the Sapphire crystal
and zirconia high temperature ability. Add to these issues, the
polarization and component alignment sensitivity of the entire frontend
sensor assembly and the Fabry-Perot cavity spectral notch/peak shape
spoiling due to varying cavity material parameters. In particular, the
Sapphire Crystal is highly birefringent and hence polarization direction
and optical alignment issues become critical.
[0005]An improved packaged design of this probe using many alignment tubes
(e.g., tubes made of Sapphire, alumina, stainless steel) was shown in Z.
Huang. G. R. Pickrell, J. Xu, Y. Wang, Y. Zhang,, A. Wang, "Sapphire
temperature sensor coal gasifier field test," SPIE. Proc. Vol. 5590, p.
27-36, 2004. Here the fiber collimator lens for light collimation and the
bulk polarizer (used in Y. Zhang, G. R. Pickrell, B. Qi, A. S. -Jazi, A.
Wang, "Single-crystal sapphire-based optical high temperature sensor for
harsh environments," Opt. Eng., 43, 157-164, 2004) are interfaced with a
commercial Conax, Buffalo multi-fiber cable with seven fibers; one
central fiber for light delivery and six fibers surrounding the central
fiber for light detection. All fibers have 200 micron diameters and hence
are multi-mode fibers (MMF). Hence this temperature sensor design is
again limited by the spectral spoiling plus other key effects when using
very broadband light with MMFs. Specifically, light exiting a MMF with
the collimation lens has poor collimation as it travels a free-space path
to strike the sensing crystal. In effect, a wide angular spread optical
beam strikes the Sapphire crystal acting as a Fabry-Perot etalon. The
fact that broadband light is used further multiplies the spatial beam
spoiling effect at the sensing crystal site. This all leads to additional
coupling problems for the receive light to be picked up by the six MMFs
engaged with the single fixed collimation lens. Recall that the best
Fabry-Perot effect is obtained when incident light is highly collimated;
meaning it has high spatial coherence. Another problem plaguing this
design is that any unwanted mechanical motion of any of the mechanics and
optics along the relatively long (e.g., 1 m) freespace optical processing
path from seven fiber-port to Sapphire crystal cannot be countered as all
optics are fixed during operations. Hence, this probe can suffer
catastrophic light targeting and receive coupling failure causing
in-operation of the sensor. Although this design used two sets of manual
adjustment mechanical screws each for 6-dimension motion control of the
polarizer and collimator lens, this manual alignment is only temporary
during the packaging stage and not during sensing operations. Another
point to note is that the tube paths contain air undergoing extreme
temperature gradients and pressure changes; in effect, air turbulence
that can further spatially spoil the light beam that strikes the crystal
and also for receive light processing. Thus, this mentioned design is not
a robust sensor probe design when using freespace optics and
fiber-optics.
[0006]Others such as Conax Buffalo Corp. U.S. Pat. No. 4,794,619, Dec. 27,
1988 have eliminated the freespace light path and replaced it with a MMF
made of Sapphire that is later connected to a silica MMF. The large
Numerical Aperture (NA) Sapphire fiber captures the Broadband optical
energy from an emissive radiative
hot source in close proximity to the
Sapphire fiber tip. Here the detected optical energy is measured over two
broad optical bands centered at two different wavelengths, e.g., 0.5 to 1
microns and 1 to 1.5 microns. Then the ratio of optical power over these
two bands is used to calculate the temperature based on prior 2-band
power ratio vs. temperature calibration data. This two wavelength band
power ratio method was described earlier in M. Gottlieb, et. al., U.S.
Pat. No. 4,362,057, Dec. 7, 1982. The main point is that this
2-wavelength power ratio is unique over a given temperature range. Using
freespace optical infrared energy capture via a lens, a commercial
product from Omega Model iR2 is available as a temperature sensor that
uses this dual-band optical power ratio method to deduce the temperature.
Others (e.g., Luna Innovations, V A and Y. Zhu, Z. Huang, M. Han, F.
Shen, G. Pickrell, A. Wang, "Fiber-optic high temperature thermometer
using sapphire fiber," SPIE Proc. Vol. 5590, pp. 19-26, 2004.) have used
the Sapphire MMF in contact with a high temperature handling optical
crystal (e.g., Sapphire) to realize a temperature sensor, but again the
limitations due to the use of the MMF are inherent to the design.
[0007]It has long been recognized that SiC is an excellent high
temperature material for fabricating electronics, optics, and
optoelectronics. For example, engineers have used SiC substrates to
construct gas sensors [A. Arbab, A. Spetz and I. Lundstrom, "Gas sensors
for high temperature operation based on metal oxide silicon carbide
(MOSiC) devices," Sensors and Actuators B, Vol. 15-16, pp. 19-23, 1993].
Prior works include using thin films of SiC grown on substrates such as
Sapphire and Silicon to act as Fabry Perot Etalons to form high
temperature fiber-optic sensors [G. Beheim, "Fibre-optic thermometer
using semiconductor-etalon sensor," Electronics Letters, vol. 22, p. 238,
239, Feb. 27, 1986; L. Cheng, A. J. Steckl, J. Scofield, "SiC thin film
Fabry-Perot interferometer for fiber-optic temperature sensor," IEEE
Tran. Electron Devices, Vol. 50, No. 10, pp. 2159-2164, October 2003; L.
Cheng, A. J. Steckl, J. Scofield, "Effect of trimethylsilane flow rate on
the growth of SiC thin-films for fiber-optic temperature sensors,"
Journal of Microelectromechanical Systems, Volume: 12, Issue: 6, Pages:
797-803, December 2003]. Although SiC thin films on high temperature
substrates such as Sapphire can operate at high temperatures, the SiC and
Sapphire interface have different material properties such as thermal
coefficient of expansion and refractive indexes. In particular, high
temperature gradients and fast temperature/pressure temporal effects can
cause stress fields at the SiC thin film-Sapphire interface causing
deterioration of optical properties (e.g., interface reflectivity)
required to form a quality Fabry-Perot etalon needed for sensing based on
SiC film refractive index change. Note that these previous works also had
a limitation on the measured unambiguous sensing (e.g., temperature)
range dictated only by the SiC thin film etalon design, i.e., film
thickness and reflective interface refractive indices/reflectivities.
Thus maker a thinner SiC film would provide smaller optical path length
changes due to temperature and hence increase the unambiguous temperature
range. But making a thinner SiC film makes the sensor less sensitive and
more fragile to pressure. Hence, a dilemma exists. In addition,
temperature change is preferably estimated based on tracking optical
spectrum minima shifts using precision optical spectrum analysis optics,
making precise temperature estimation a challenge dependent on the
precision (wavelength resolution) of the optical spectrum analysis
hardware. In addition, better temperature detection sensitivity is
achieved using thicker films, but thicker etalon gives narrower spacing
between adjacent spectral minima. Thicker films are harder to grow with
uniform thicknesses and then one requires higher resolution for the
optical spectrum analysis optics. Hence there exists a dilemma where a
thick film is desired for better sensing resolution but it requires a
better precision optical spectrum analyzer (OSA) and of course thicker
thin film SiC etalons are harder to make optically flat. Finally, all to
these issues the Fabry-Perot cavity spectral notch/peak shape spoiling
due to varying cavity material parameters that in-turn leads to
deterioration in sensing resolution.
[0008]Material scientists have also described non-contact laser assisted
ways to sense the temperature of optical chips under fabrication. Here,
both the chip refractive index change due to temperature and thermal
expansion effect have been used to create the optical interference that
has been monitored by the traditional Fabry-Perot etalon fringe counting
method to deduce temperature. These methods are not effective to form a
real-time temperature sensor as these prior-art methods require the
knowledge of the initial temperature when fringe counting begins. For
industrial power plant applications, such a prior knowledge is not
possible, while for laboratory material growth and characterization, this
a prior knowledge is possible. As shown later in this application, our
described sensor designs solve this problem and no longer need the
initial temperature data as real-time fringe counting is not used. Prior
works in this general laser-based materials characterization field
include: F. C. Nix & D. MacNair, "An interferometric dilatometer with
photographic recording," AIP Rev. of Scientific Instruments (RSI)
Journal, Vol. 12, February 1941; V. D. Hacman, "Optische Messung der
substrat-temperatur in der Vakuumaufdampftechnik," Optik, Vol. 28, p 115,
1968; R. Bond, S. Dzioba, H. Naguib, J. Vacuum Science & Tech., 18(2),
March 1981; K. L. Saenger, J. Applied Physics, 63(8), Apr. 15, 1988; V.
Donnelly & J. McCaulley, J. Vacuum Science & Tech., A 8(1),
January/February 1990; K. L. Saenger & J. Gupta, Applied Optics, 30(10),
Apr. 1, 1991; K. L. Saenger, F. Tong, J. Logan, W. Holber, Rev. of
Scientific Instruments (RSI) Journal, Vol. 63, No. 8, August 1992; V.
Donnelly, J. Vacuum Science & Tech., A 11(5), September/October 1993; J.
McCaulley, V. Donnelly, M. Vernon, I. Taha, AIP Physics Rev. B, Vol. 49,
No. 11, 15 Mar. 1994; M. Lang, G. Donohoe, S. Zaidi, S. Brueck, Optical
Engg., Vol. 33, No. 10, October 1994; F. Xue, X. Yangang, C. Yuanjie, M.
Xiufang, S. Yuanhua, SPIE Proc. Vol. 3558, p. 87, 1998.
SUMMARY DESCRIPTION OF THE INVENTION
[0009]Ideally, one would like a robust optical sensor that can be remoted,
is minimally invasive, works at high temperatures (e.g., 2000.degree. C.)
and pressures including chemically corrosive environments, requires low
cost low loss optics, has high sensing resolution over any extended wide
unambiguous range, and provides easy access to many sensing points. In
commonly assigned U.S. patent application Ser. No. 11/185,540
incorporated herein by reference, modules for the needed extreme
environment minimally invasive optical free-space laser beam targeted
optical sensor using preferably single crystal Silicon Carbide (SiC)
optical sensor chip(s) acting as a natural Fabry-Perot Etalon(s) are
described. A key point in these designs is that laser light is launched
into freespace using a Single-Mode Fiber (SMF); hence the light beam
striking the temperature sensing SiC crystal has excellent spatial
coherence (or collimation properties), making the optically sensed
reading highly accurate and sensitive. The present application describes
robust optical probe designs for these earlier described SiC single
crystal optical sensors, including novel techniques for measurement of
refractive index, temperature, pressure, and thickness.
[0010]This application describes self-calibrating and aligning aspects of
the probe design via the use of SMF optics. Specifically, the SMF acts as
a confocal optical system that insures that the sensor is properly
aligned and hence providing the correct sensing data. It is shown that
for a given fixed temperature, the described sensor set-up can provide
accurate optical sample thickness measurements using the known Sellmeier
equation (that gives the wavelength dependent refractive index) for the
given sample. Similarly, knowing the sample thickness, the sample
Sellmeier equation can be found.
[0011]Mechanical motion of alignment mirrors have been described to keep
the freespace laser beam targeting on the SiC chip and receive optical
detector. In the present application, described is a simpler non-mirror
electronically actuated mechanical alignment assembly technique for the
SMF-Lens combination so the sensor probe can implement fast real-time
alignment operations for the free-space beam striking the sensing SiC
single crystal that is acting as a temperature sensor. In other words,
using for example fine tilt control piezo-electric motion control
mechanics on the entire SMF-Fiber lens (FL) assembly, one can accurate
point the laser beam (LB) to the correct retroreflective position on the
SiC chip, thus enabling robust temperature probe design in harsh
environments.
[0012]Described are packaged probe designs using laser-bonded single
crystal SiC chip on-to a SiC (e.g., re-crystallized SiC) tube assembly
that provides an excellent match of the SiC tube and SiC single crystal
material Coefficients of Thermal Expansions (CTEs), hence preventing
breaking of the SiC chip due to extreme temperature swings. Also provided
is a vacuum sealed tube design using a glass window made for example from
low CTE Borosilicate Glass (called Pyrex by Coming) or low CTE (0.55
microns/meter-deg. C.) synthetic fused silica or BK7 Glass (Schott
Glass). Key points to note is that the SiC tube materials (e.g.,
polycrystalline SiC) has a lower Coefficient of Thermal Conductivity
(CTC: units W/m-K of 33 to 270 W/K-m)) than high optical quality single
crystal SiC (CTE: 330 W/K-m), yet both have similar CTEs around 4.2 to
4.68 ppm/K. This helps in preventing heat transfer from the
hot chip end
of the tube to the glass window end of the tube. Further low CTC tubing
such as made from ceramics such as Alumina Al.sub.2O.sub.3 or Silicon
(CTC: 150 W/K-m) is also used from the glass window edge to the cooler
insertion point zone of the probe where the alignment and launch-receive
optics sits in an ambient (e.g., <65.degree. C.) temperature chamber.
The described probe can also use convention cooling on the tubing near
the transmit/receive fiber and bulk optics assembly to keep temperatures
down to <65.degree. C. in the optical enclosure, as typically needed
for SMF optics. Such a probe is ideal for power plant systems where
extreme temperatures range from 1400.degree. C. to 1600.degree. C. in the
hot zones of combustion chambers that are near a meter inside the chamber
with chamber wall temperatures around 300.degree. C. to 500.degree. C.
Using a variety of SiC tubes and other low CTC ceramic tubes, various
probe designs (see FIG. 3-4) are described for extreme temperature,
pressure, and corrosion conditions.
[0013]Described in FIG. 5 is a multi-tip probe design using multiple
independent SiC crystal chips in separate SiC tubes all encased in one
larger SiC tube to enable fault-tolerant and self-calibrating sensing.
[0014]An example application of the described hybrid SMF-freespace
temperature probe shown in FIG. 6 is a temperature sensing probe for
moving parts such as a wheel of an aircraft landing gear or a turbine
blade in a aircraft engine or power generation system. Described is an
assembly to meet these temperature sensing requirements when temperature
of a moving part is to be determined. Here, if needed, one can use a
higher power laser to burn-off any debris and the infrared (IR) red laser
to read the moving part temperature.
[0015]FIG. 7 shows an alternate mounting condition for the SiC chip that
is less effected by pressure differentials between the two faces of the
chip.
[0016]Described also is a probe design in FIG. 8 that can simultaneously
measure temperature and pressure using localized optical beam targeting
for temperature sensing and spatial or global optical targeting of SiC
crystal chip for pressure sensing via optical interference pattern
detection and processing.
[0017]General applications for the described sensor include use in fossil
fuel-based power systems, aerospace/aircraft systems, satellite systems,
deep space exploration systems, and drilling and oil mining industries.
In other words, both extremely hot or extremely cold conditions can use
the described temperature probes. In fact, cold conditions tend to be
more inert and stable and hence one can expect exceptional performance
from the described SiC chip and tube-based probes.
[0018]An optical pressure sensor can be designed when using a High
Pressure Capsule (HPC) design where the HPC uses the single crystal SiC
chip as an optical window accessed by a laser beam. The HPC can be made
with the sintered SiC material so CTE's of chip/window and HPC material
are matched to prevent thermal deformation effects on the chip. The
sensors can also be designed into small fiber-optic packages.
DESCRIPTION OF THE DRAWINGS
[0019]FIG. 1 shows an example embodiment of etalon measurement system
using hybrid freespace-fiber optics and wavelength selective
interferometry and processing.
[0020]FIG. 2 shows another example embodiment of a high spatial resolution
etalon measurement system design using an imaging type GRIN fiber lens.
[0021]FIG. 3 shows another example embodiment for a probe package design
using SiC and low thermal conductivity tubes.
[0022]FIG. 4. shows another example embodiment for a probe design using
SiC tube-on-tube protection.
[0023]FIG. 5. shows an example embodiment for a Fault-tolerant
self-Calibrating probe design.
[0024]FIG. 6. shows an example embodiment for a Wireless fault-tolerant
probe design for moving parts temperature sensing.
[0025]FIGS. 7a-7b show an example embodiments of a mounting mechanism for
the SiC crystal chip on (a) a SiC tube and (b) a SiC substrate mount
using laser bonding.
[0026]FIG. 8 shows an example embodiment for a design of simultaneous
temperature and pressure sensing probe.
[0027]FIG. 9 shows an example embodiment of a SiC-chip based remote
wireless optical pressure sensor.
[0028]FIG. 10 shows a Weak Lens (WL) optical ray-trace model that
describes how the SiC chip acts as a pressure dependant concave lens that
diverges and magnifies the input laser beam.
[0029]FIGS. 11a-11b show an example embodiments of a compact
fiber-connected SiC frontend sensor designs for (a) temperature and (b)
pressure sensing.
[0030]FIG. 12 shows an example embodiment of a packaged pressure-only
sensor design for long range access of hot zone.
[0031]FIG. 13 shows an example embodiment of a Wireless Hybrid Optical
Sensor for Simultaneous Temperature and Pressure Measurements for short
access points.
DETAILED DESCRIPTION OF THE INVENTION
[0032]Knowing the exact thickness of optical components is a critical need
when designing high quality large, miniature, and super small optics for
numerous platforms such as integrated-waveguide optics, bulk-optics, and
fiber-optics. Over the years, many methods have been described to measure
thickness from the thin-film level (i.e., smaller than the optical
wavelength) to thick plates (i.e., hundreds of wavelengths). Perhaps the
most tried method is based on the classic Michelson optical
interferometry using a broadband optical source such as white light [see
P. A. Flourney, R. W. McClure, G. Wyntjes, "White light interferometric
thickness gauge," Appl. Opt., 11, 1907 (1972); L. M. Smith and C. C.
Dobson, "Absolute displacement measurements using modulation of the
spectrum of white light in a Michelson interferometer," Appl. Opt., 28,
3339 (1989)]. Here, the short coherence length of the broadband source is
used to produce interferometer arms path-length difference-based output
detected white light fringes that are processed to obtain the sample
thickness measurement. These white light fringes can be captured in the
time domain by scanning a reference mirror over a known scan range and
recording the fringe power, with the maximum optically detected power
position giving data to calculate the sample thickness. This method has
also been called low coherence reflectometry or time domain optical
coherence tomography (OCT) [see R. C. Youngquist, S. Carr, and D. E. N.
Davies, "Optical coherence-domain reflectometry: a new optical evaluation
technique," Opt. Lett. 12, 158 (1987); K. Takada, I. Yokohama, K. Chida,
and J. Noda, "New measurement system for fault location in optical
waveguide devices based on an interferometric technique," Appl. Opt., 26,
1603 (1987); M. Haruna, M. Ohmi, T. Mitsuyama, H. Tajiri, H. Maruyama,
and M. Hashimoto, "Simultaneous measurement of the phase and group
indices and the thickness of transparent plates by low-coherence
interferometry," Opt. Lett. 23, 966 (1998)].
[0033]An alternate twist to white light interferometry is wavelength
scanning interferometry where the broadband source is produced in time by
tuning a laser and the interferometer output is observed on a per
wavelength basis [see Y. Ishii, J. Chen, and K. Murata, "Digital
phase-measuring interferometry with a tunable laser diode," Opt. Lett.,
12, 233 (1987); M. Suematsu and M. Takeda, "Wavelength-shift
interferometry for distance measurements using the Fourier transform
technique for fringe analysis," Appl. Opt., 30, 4046 (1991); F. Lexer, C.
K. Hitzenberger, A. F. Fercher, and M. Kulhavy, "Wavelength-tuning
interferometry of intraocular distances," Appl. Opt., 36, 6548 (1997); K.
Hibino, B. F. Oreb, P. S. Fairman, and J. Burke, "Simultaneous
measurement of surface shape and variation in optical thickness of a
transparent parallel plate in wavelength scanning Fizeau interferometer,"
Appl. Opt., 43, 1241 (2004)].
[0034]For instance, the interferometer output can be dispersed into
spatially independent bins representing different wavelengths along a
linear detector array. In this case, by Fourier transforming the
spatially observed optical spectrum, the sample thickness is determined
without using any motion of the reference mirror or sample along the
optical axis. In a similar fashion by temporally sweeping the laser
wavelength and temporally Fourier transforming the fringe data, one can
determine the sample optical thickness. This Fourier domain approaches
are now be referred to as spectral domain OCT. Even ultra-fast light in
the TeraHertz (THz) bandwidth range has been described for measuring
optical thickness [see F. Huang, J. F. Federici, and D. Gary,
"Determining thickness independently from optical constants by use of
ultrafast light," Opt. Lett. 29, 2435-2437 (2004)].
[0035]As is clear with the previously mentioned techniques that are
considered fore-runners in thickness measurement instruments, one must
use broadband light of the widest optical spectrum, as the shorter the
coherence length, the finer the resolution of the thickness measurement.
This in-turn puts an extreme performance requirement on all components
used to assemble the interferometer (e.g., Michelson, Fizeau); in
particular, material dispersion effects in the optical components can
become significant, not to mention increased non-linear effects arising
from non-perfect linear tuning of the laser. In addition, interference
fringe power data is acquired across the entire optical spectrum to
enable the best approximation of the sample thickness. Thus, the broader
the spectrum to get a better measurement resolution, more data points are
needed to obtain this resolution. Finally and most importantly, a
fundamental limit with these broadband interferometric measurement
methods is that they ignore the test sample material dispersion effects
and hence indeed are only approximations to the real sample thickness. In
fact, the instrument designer faces a dilemma where a broader spectrum is
expected to give the better measurement resolution but at the same time
will add more component and sample material dispersion effects to the
measurement, hence reducing the accuracy of the measurement.
[0036]In this application, described is a solution to eliminate the
effects of using very broadband light, whether in the interferometer
optics or the sample. First, described is the use of a direct free-space
material dispersion-free laser beam to interrogate the test sample in air
that is expected to naturally act as the interferometer via the
Fabry-Perot effect. Thus removed is the need for many material
dispersion-free optical components required to assemble for example a
Michelson interferometer. Second, described is the use of only a few
(e.g., five) closely spaced accurately measured discrete wavelengths,
thus removing the need to acquire optical power data over a very broad
continuous optical spectrum. Third, sample refractive index data at only
the chosen few (e.g., five) adjacent wavelengths is needed for
processing. Note that today extensive and accurate material dispersion
data in the form of the Sellmeier equation is available for key optical
substrate materials such as Silicon (Si) [see D. F. Edwards, "Silicon
(Si)", in E. D. Palik (Ed.), Handbook of Optical Constants of Solids,
Inc., 547 (Academic Press 1985)] and Silicon Carbide (SiC) [see W.
Martienssen and H. Warlimont, Eds., Handbook of Condensed Matter and
Materials Data, XVII (Springer 2005)]. Fourth, the described thickness
calculation uses a closed form expression based on Fabry-Perot
interferometry; hence providing an exact measured value for the sample
thickness. Finally, the use of a Single Mode Fiber (SMF) coupled to fiber
lens optics insures a confocal self-aligning set-up and hence provides
the launching and reception of a high collimation on-axis wireless
optical beam needed for proper sample access. In effect, the described
system is self-calibrating and insures a true thickness measurement. The
rest of the application describes the described thickness (or temperature
or refractive index) measurement hybrid fiber-freespace system design.
Such a system is ideal for measuring the large thickness of sample wafers
such as Si and 6H--SiC Crystals such as recently described to form
wireless optical sensors for temperature sensing [see U.S. patent
application Ser. No. 11/185,540 and N. A. Riza, M. A. Arain, and F.
Perez, "Harsh Environments Minimally Invasive Optical Sensing Technique
for Extreme Temperatures: 1000.degree. C. and Approaching 2500.degree.
C.," in Proceedings of the 17.sup.th Optical Fiber Sensors Conference,
(SPIE 2005) Vol. 5855, p. 687; N. A. Riza, M. A. Arain, and F. Perez,
"Harsh Environments Minimally Invasive Optical Sensor using Freespace
Targeted Single Crystal Silicon Carbide," IEEE Sensors J., accepted
(2005); N. A. Riza, M. A. Arain, and F. Perez, "6-H Single Crystal
Silicon Carbide Thermo-optic Coefficient Measurements for Ultra High
Temperatures up to 1273 K in the Telecommunications IR band," J. Appl.
Phys., 98, (2005)]. FIG. 1 shows the described hybrid fiber-freespace
thickness sensor system that is based on this earlier high temperature
freespace targeted temperature sensor design. Because this system relies
on the natural Fabry-Perot interferometry produced by the sample placed
in air (and if needed vacuum), the optical sample must be a
non-scattering partially reflecting (or semi-transparent) parallel-plate
structure over the optical observation spot. Earlier, a multi-beam
interference approach for thickness measurements was described that was
focused on using broadband light for thin-film (<.lamda.) thickness
measurements for films on thick substrates [see R. Swanepoel,
"Determination of the thickness and optical constants of amorphous
silicon," J. Phys. E: Sci. Instrum. 16, 1214 (1983)]. This study
concluded that direct use of all the wideband spectra optical power
maxima (or minima) and related wavelength values is not a very accurate
method for measuring the thin film thickness. In fact, it was correctly
shown that although multi-beam interferometry provides an exact closed
form expression for the sample thickness, the technique is extremely
sensitive to the sample material dispersion data and requires further
optical data and processing to produce better accuracy results [see R.
Swanepoel, "Determining refractive index and thickness of thin films from
wavelength measurements only," J. Opt. Soc. Am. A, 2, 1339 (1985)]. A key
reason for this limitation was the thin-film nature of the sample that
caused a large (e.g., 45 nm) separation between adjacent spectra maxima
(or minima). This large wavelength separation translated to a large
(e.g., 0.05) refractive index change for the adjacent wavelength
positions for the used amorphous silicon material.
[0037]In addition, these earlier multi-beam interferometry methods
provided no instrument self-calibration (or self-alignment) method so the
placement of the sample guaranteed a true thickness reading. In an aspect
of the invention, an example method for measuring a thickness of an
etalon may include directing a first light beam at a first frequency and
a second light beam at a second frequency at a first portion of an etalon
having a known characteristic and receiving the first light beam and the
second light beam from the etalon. The method may also include
identifying a first condition of the first light beam and a second
condition of the second light beam received from the etalon; and
calculating a first thickness of the etalon responsive to the first
condition, the second condition, and the known characteristic. The first
condition may include at least one of an interference maximum and an
interference minimum of the first light beam and the second condition may
include at least one of an interference maximum and an interference
minimum of the second light beam. The method may further include
determining respective refractive indices of the etalon for the at least
one of the interference maximum and the interference minimum of the first
light beam and for the at least one of the interference maximum and the
interference minimum of the second light beam, such as by using the known
Sellmeier equation and then calculating the thickness according to
equation (2) above.
[0038]The described FIG. 1 system solves these problems by using a hybrid
design that uses both fiber and free-space optics and etalons such as Si
and 6H--SiC whose material dispersion data via the Sellmeier equations
are accurately available in the literature [see D. F. Edwards, "Silicon
(Si)", in E. D. Palik (Ed.), Handbook of Optical Constants of Solids,
Inc., 547 (Academic Press 1985); W. Martienssen and H. Warlimont, Eds.,
Handbook of Condensed Matter and Materials Data, XVII (Springer 2005)].
Furthermore, the typical mentioned Si and 6H--SiC substrates are thick
(d>>probe wavelength .lamda., e.g., d=300 .mu.m) leading to small
inter-wavelength gaps (e.g., <2 nm) that reduces thickness measurement
errors due to inaccuracies in prior reported wavelength dependent
refractive index data. These sample conditions are indeed met for the
concerned temperature sensor applications using Si and SiC substrates.
[0039]The FIG. 1 system 10 uses two optical processing trains. First, a
moderate bandwidth (e.g., 10 nm) broadband source 12 directs light beams
at the sample 26, such as an etalon, via control of a 2.times.1
fiber-optical switch 14. Light beams from the broadband source 12 pass
via the switch 14 to enter a fiber-optic circulator 16 that directs the
light via an SMF 18 to a fiber lens 20. This fiber lens 20 is a special
Gradient Index (GRIN) lens that produces an output Gaussian beam 30 with
its minimum beam waist 24 located at a distance d from the output GRIN
lens surface 22. The location of the freespace beam waist 24 also marks
the location of the sample plane. Note that this minimum beam waist 24
location is also where the laser beam has near perfect collimation, a
condition required for high quality Fabry-Perot interferometry. Hence,
plane waves are launched into the parallel faces of the sample 26 at the
localized minimum beam waist 24 spot. To profile the entire sample 26,
the sample 26 is physically translated in the plane of the beam
cross-section by translation element 40 or stage. For high accuracy
thickness measurements, the beam 30 must strike at normal incidence on
the sample 26. In the described system, this is naturally achieved by
aligning the sample 26 to maximize the received optical power coupled
back into the SMF 18. In other-words, only when the sample acts like a
retro-reflecting surface in the minimum beam waist 28 plane of the
incident beam 30 does one get the lowest freespace-to-SMF coupling loss
[see M. van Buren and N. A. Riza, "Foundations for low loss fiber
gradient-index lens pair coupling with the self-imaging mechanism,"
Applied Optics, Appl. Opt., 42, 550 (2003)]. Thus by monitoring the
received optical power, one can conclude that the sample 26 is correctly
aligned for a true thickness measurement. This same principle is also
true for a true temperature (or refractive index) measurement via the
optical chip (e.g., SiC crystal) used in the FIG. 1 system that acts as a
freespace laser beam targeted temperature sensor.
[0040]Because the sample refractive index and optical loss due to all
system components is known, one can use Fresnel reflection coefficient
theory to estimate the maximum optical power reflected from a given
substrate. Hence, knowing the total expected losses from all components
in the system including a test sample, one can approximate the expected
optical power detected when the sample 26 is correctly aligned. In short,
the described system provides the self-calibration feature needed for
true measurements via classic Fabry-Perot interferometry. This maximized
light re-coupled into the SMF 18 passes via the circulator 16 and another
fiber-optic 1.times.2 switch set 32 such that the sample reflected
broadband light enters an optical receiver, such as fiber-coupled optical
spectrum analyzer 34. The nature of the used broadband source is to
provide a few observable interference fringes for the output spectrum.
Hence, perhaps two to 5 fringes are needed to add a 2 to 5 redundancy
into the described thickness measurement. Hence, unlike previous
approaches that rely on extensive broadband data over continuous and very
wide spectra, the described sensor only needs spectra data over a narrow
(e.g., 10 nm) range. Specifically, the OSA 34 is used to read the
wavelength location of say 5 fringe minima positions. The accuracy of the
wavelength reading depends on the resolution of the OSA 34, both in terms
of wavelength and optical power reading. Thus, using the broadband source
and OSA 34, a first reading of wavelength positions is noted. Next, the
two optical switches 14, 32 in the FIG. 1 system are flipped and a
tunable laser 36 and optical power meter 38 are switched into the
measurement system 10 to take a second reading for wavelength positions.
Here the tuning resolution of the laser 36 combined with the accuracy of
the power meter 38 will determine the accuracy of the taken wavelength
readings. Hence, two sets of wavelength readings can be taken to add
fault-tolerance to the measurement system. Pairs of these adjacent
spectral minima readings in conjunction with the pre-known sample
refractive index data via the known Sellmeier equations is then used to
compute the sample thickness value at the given probed sample location
set by the mechanical translation stage.
[0041]It is well known that the optical power reflectance from a
Fabry-Perot cavity is given by:
R FP = R 1 + R 2 + 2 R 1 R 2 cos .phi.
1 + R 1 R 2 + 2 R 1 R 2 cos .phi. ,
( 1 )
where R.sub.1 and R.sub.2 are the Fabry-Perot etalon front and back mirror
reflectances, respectively. .phi. is the round-trip propagation phase
accumulated by an optical beam while passing through the sample etalon of
thickness t and refractive index n(.lamda.) at a wavelength of .lamda.,
and is given by
.phi. = 4 .pi. n ( .lamda. ) t .lamda.
at normal incidence. For the test substrate sample in air,
R.sub.1=R.sub.2=R=r.sup.2, where r=[n(.lamda.)-1]/[n(.lamda.)+1] is the
Fresnel amplitude reflection coefficient of an air-sample interface. Eq.
1 indicates that the maximum reading of the described FIG. 1 system are
taken when cos(.phi.)=1 or .phi.=2.pi.m, where m=0, 1, 2, 3, . . . ,
while the minimum reading of the received optical power are taken when
cos(.phi.)=-1 or .phi.=(2m-1).pi.. Hence, as the wavelength .lamda. of
the system optical source engaging the sample changes from one spectrum
minimum (or maximum) position to the adjacent minimum position, the
optical path length in the substrate has changed causing .phi. to change
by 2.pi. radians. Given that the first chosen power minimum occurs at a
measured .lamda..sub.1, the sample round-trip propagation phase
accumulated is given by:
.phi..sub.1={4.pi.n(.lamda..sub.1)t/.lamda..sub.1}. Similarly, for the
adjacent power minimum occurring at a measured .lamda..sub.2 value, the
sample round-trip propagation phase accumulated is given by:
.phi..sub.2={4.pi.n(.lamda..sub.2)t/.lamda..sub.2}. Given that for any
two chosen adjacent spectra power minima with
.lamda..sub.2>.lamda..sub.1 the roundtrip optical phase changes by
2.pi., .phi..sub.1-.phi..sub.2 can be written to give the sample
closed-form exact optical thickness value t of:
t = .lamda. 1 .lamda. 2 2 ( .lamda. 2 n 1 -
.lamda. 1 n 2 ) , ( 2 )
where n(.lamda..sub.1)=n.sub.1 and n(.lamda..sub.2)=n.sub.2.
[0042]The sample substrate cuts can be chosen such that the material has
one refractive index in the plane containing the linear polarization and
these refractive indices are given by the following Sellmeier equations:
[0043]For 6H:SiC (ordinary index);
n 2 ( .lamda. ) = A + B .lamda. 2 .lamda. 2 -
C , ( 3 )
where A=1, B=5.5515, C=0.026406, and .lamda. is in .mu.m. In particular,
the crystal or c-axis for the given 6H--SiC chip is along the optical
beam propagation direction and the crystal ordinary index is given to be
normal to the crystal c-axis. Hence the incident linear polarization sees
the given ordinary index in Eqn. 3 for the 6H--SiC chip.
[0044]For Si,
n 2 ( .lamda. ) = + A .lamda. 2 + B .lamda. 1
2 .lamda. 2 - .lamda. 1 2 , ( 4 )
where .lamda..sub.1=1.1071 .mu.m, .epsilon.=11.6858, A=0.939816,
B=0.00810461, and .lamda. is in .mu.m.
[0045]Do note from FIG. 2 that improved localized thickness measurements
are possible using a focused probe beam such as from a 0.29 pitch imaging
type fiber GRIN lens 21. In conclusion, this application shows that high
measurement accuracy from the described thickness measurement sensor is
possible given the high performance of today's state-of-the-art
wavelength tunable lasers, optical spectrum analyzers, optical power
meters, fiber-optics, optical chip fabrication methods, and well
documented optical material dispersion data. The described method
provides a simple, self-calibrating, non-contact mechanism for accurate
optical chip thickness measurements such as needed for sensors based on a
variety of optical crystal chips.
[0046]According to the description above, in an example embodiment, a
system for measuring a thickness of an etalon may include a first light
source, e.g., tunable laser 36 or broadband light source 12, for
directing a first light beam having a first wavelength at a first portion
of an etalon having a known characteristic and a second light source
e.g., tunable laser 36 or broadband light source 12, for directing a
second light beam having a second wavelength different from the first
wavelength at the etalon, e.g. sample 26. The system may also include an
optical receiver, such as optical spectrum analyzer 34 or power meter 38,
for receiving the first light beam and the second light beam from the
etalon and for providing a first power signal corresponding to the first
light beam received from the etalon and a second power signal
corresponding to the second light beam received from the etalon. The
system may also include a processor 42 for identifying a first condition
of the first power signal and a second condition of the second power
signal received from optical receiver and calculating a thickness of the
etalon responsive to the first condition, the second condition, and the
known characteristic.
[0047]For extreme temperature, pressure, and corrosive fluid/gas species
environments, the FIG. 1 and FIG. 2 sensing/measurement systems require
appropriate probe designs and packaging. For these extreme environments,
an insertion-type probe design is described in FIG. 3 where the sensor
probe 44/stick is inserted into the harsh sensing zone 46 via an inlet
with a sealed gasket G1 48 and fitting FT 50 on the probe engaging
another high pressure gasket and fitting in the chamber wall inlet. The
sensing chamber gasket & fitting couples with the sealed gasket-fitting
G1 48-FT 50 on the probe 44, making a temperature, pressure and gas
isolating interface between the extreme sensing environment 46 (e.g.,
combustion chamber, turbine engine, etc) and external ambient environment
52 where instrument controls and technicians operate and service the
industrial systems. A typical extreme or
hot zone temperature T1 a
certain distance equivalent to the L1+L2+L3/2 length of probe (e.g., 100
cm) inside the chamber away from the internal wall 54 might be
T1=1600.degree. C., while the temperature at the chamber internal wall 54
might be T2=600.degree. C. At the exterior wall 56 location, the
temperature T3 will be lower (e.g., 400.degree. C.) compared to the
interior wall 54. Further, the probe temperature T4 a certain distance L3
away from the exterior wall 56 and in the ambient conditions (e.g.,
60.degree. C. temperature) environment will be a much lower value, e.g.,
T4=200.degree. C., due to thermal cooling due to ambient air convection
and thus heat transfer over the probe surface. This T4 to T3 temperature
range probe length can have a typical, e.g., L4+L3/2=30 cm length in the
ambient conditions zone 52 so it is away from the chamber wall hot zone
46 and hence safer for handling. An additional thermally insulating probe
section 60 Of length L5 (e.g., 10 cm) is added to take the probe
temperature down from T4 to T5 where T5 is the ambient temperature, e.g.,
T5=60.degree. C.). This T5 temperature section of the probe 44 is the
probe terminal head section "H" 62 that contains a light directing
element, or probe transmit and receive beam conditioning and control
optics 63. The total probe length from hot zone tip portion 64 to head
portion 62 can be estimated to be L1+L2+L3+L4+L5, e.g., 140 cm. Hence,
the freespace light beam 66 must travel a distance L1+L2+L3+L4+L5 (e.g.,
about 140 cm) to strike an etalon, for example, 6H--SiC sensor
crystal/chip 68. For the extreme hot temperature conditions, the hotter
probe sections from temperature T1 to T4 (or lengths L1+L2+L3+L4) are
vacuum sealed to prevent air turbulence inside the probe 44 that can
spatially spoil the laser beam 66 to and from the SiC chip 68. The use of
a vacuum in the sealed SiC is a design option for reducing possible beam
spoiling/wander effects on the laser beam 66 in case the tube is
containing air. The L5 section made for a low CTC material can contain
air under favorable ambient conditions with minimal turbulence.
Alternately, the entire length of the probe 44, i.e., L1+L2+L3+L4+L5 can
be vacuum sealed to insure that no air turbulence affects the propagating
a light beam, such as freespace laser beam 66.
[0048]SiC tubes (labeled as ST's in the FIGS. 3-7) may be made of a
variety of SiC material forms (see Morgan Advanced Ceramics/HaldenWanger,
Germany) such as Halsic-R (recrystallized SiC), Halsic-I (silicon
infilterated SiC), Halsic-S (sintered SiC), Halsic-RX (recrystallized and
doped SiC). Some of these SiC tubes are porous (e.g., Halsic-R) while
others (e.g., Halsic-S) are impermeable to gases. Hence, also described
is possible use of the porous-type SiC tubes for gas species optical
sensing using the described freespace laser beam sensor probe designs.
For vacuum seal tube designs, the impermeable SiC tubes are required for
probe assembly. If sealing of SiC tubes is not essential for the
described probe design under given applications, then one can deploy the
porous SiC tubes for probe assembly. Typically, commercial SiC tube are
available with lengths up-to 3 m and outer-diameters ranging from 15 mm
to 80 mm and inner diameters ranging from 5 mm to 66 mm. Hence, as shown
in FIG. 3, a SiC tube e.g. 70a can be inserted into another SiC tube e.g.
70b to enable longer probe lengths and probes with large surface area for
heat dissipation. For the lower CTC high insulation tubes labeled as "I"
tubes 60 to house the optics 63, other ceramic materials can be used such
as alumina (see Morgan Technical Ceramics, Catalog, Fairfield, N.J., USA)
or sheath materials such as Tantalum, Molybdenum, Platinum/Rhodium,
Inconel 600, Nickel-Chrome based Super OMEGACLAD XL and insulators such
as Hafnium Oxide, Magnesia, and Alumina (see Omega Exotic Thermocouple
Probes Catalog, Stamford, Conn., USA). Depending on the porosity of the
SiC tube used for the described probe design, the quality of the vacuum
sealing will vary. To make sure excellent vacuum sealing is possible if
needed, one can encase the entire SiC tube 70a-70e and related optics 63
in one larger non-porous tube such as made of stainless steel that will
realize a high quality vacuum seal.
[0049]In FIG. 3 and related described designs, optics may be mounted on a
thermally stable substrate Base Plate B 72 with appropriate low CTE and
CTC materials. FIG. 3 and later related designs use a Single Mode Fiber
(SMF) 74 coupled to a collimating Fiber Lens (FL) 76, with alignment
mechanism, such as a tip/tilt element and/or a translation element,
controlled precisely by a piezoelectric motion stage 78 coupled to the FL
76. This piezoelectrically controlled FL 76 is critical for exactly
targeting the center of the SiC crystal chip C 68 a distance
L1+L2+L3+L4+L5 from the lens. More importantly, the piezoelectrically
controlled FL tip/tilt position makes sure the laser beam 66 produces a
retroreflective or collinear beam that can be coupled back into the SMF
74. Hence, as in designs in FIGS. 1 & 2, the FIG. 3 probe 44 is
self-aligning and self-calibrating as only for the correct
tip/tilt/translation setting of the FL 74 will produce the correct power
of the receive coupled light into the SMF, this insuring that the sensor
is correctly calibrated. In addition, if there are unwanted mechanical
vibrations in the probe, the long length of the freespace laser beam path
67 will not be a limitation as active laser beam alignment is present in
the described probe 44. Also, hitting the correct spot on a target
etalon, such as the SiC chip 68, for all temperature readings is
important because the chip 68 has a given thickness and refractive index
change behavior with temperature given its specific packaging with the
SiC tube ST1 70a and ST5 70e. As the probe 44 is calibrated for a given
laser beam hit location on the SiC chip 68, the same location must be
struck during all operations of the probe 44. There are a number of
companies that make precision motion controls using piezoelectric
ceramics for fiber-optical alignment. These include ultrafast piezo
tip/tilt platform and Z (on axis) positioner Model S-325 from Physik
Instruments (PI), Auburn, Mass., USA (and Germany), 2-axis tilter stages
from Piezo Systems, Inc., Cambridge, Mass., and Nano-MTA series tip/tilt
actuators from Mad City Labs, Madison, Wis. In short, the described probe
44 may use a state-of-the-art tip/tilt motion stage to make sure the
laser beam 66 is correctly aligned in the insulation I 60 and SiC ST
tubes 70a-70e and also strikes the SiC crystal chip C 68 for perfect
retro-reflective beam operations. SMF-FL freespace alignment constraints
and quantified limits has been earlier reported in Martin van Buren and
N. A. Riza, "Foundations for low loss fiber gradient-index lens pair
coupling with the self-imaging mechanism," Applied Optics, LP, Vo. 42,
No. 3, Jan. 20, 2003. and Shifu Yuan and N. A. Riza, "General formula for
coupling loss characterization of single mode fiber collimators using
gradient-index rod lenses," Applied Optics, Vol. 38, No. 15, pp.
3214-3222, May 20, 1999. Erratum, Applied Optics, Vol. 38, No. 30, p.
6292, October 1999. Light launched from the SMF-FL can preferably use the
self-imaging condition in Martin van Buren and N. A. Riza, "Foundations
for low loss fiber gradient-index lens pair coupling with the
self-imaging mechanism," Applied Optics, LP, Vo. 42, No. 3, Jan. 20,
2003, this making sure of high coupling efficiency for receive light back
into the SMF. Note FIG. 3 only shows the SMF 74, although as in FIG. 1
and FIG. 2, the SMF 74 is connected to other optics such as a fiber-optic
circulator, tunable and broadband laser, switches, OSA, and optical power
meter and data processor. For alignment purposes, one can tune the laser
to get maximum light power back into the SMF 74 to simulate constructive
interference in the Fabry-Perot effect in the SiC chip 68 under probe
calibration conditions. Along with the SMF 74, an electrical cable E 80
is connected to the piezo-motion stage M 78 for controls of the stage 78.
One can envision simultaneously using a visible light laser for alignment
purposes while the infrared laser for the temperature sensing operations.
Appropriate optical filters may be used at the receive optics to prevent
any unwanted optical bands from saturating or adding noise to the
photodetection process such as via Black-body thermal radiation. The SMF
74 and E 80 are in a protective cable PC 82 that has a gasket and fitting
inside the I-tube to keep the optical chamber isolated and clean. The
optical bench has an optional high extinction ratio polarizer optic 84
such as a calcite crystal polarizer that can improve interference fringe
visibility off the SiC chip 68. One can also use a polarization
maintaining SMF and hence remove the need for the polarizer P 84 in the
probe Head H 62. The SiC tube ST4 70d is closed with an optional glass
window W1 86 that makes the SiC tube assembly e.g. 70a-70e vacuum tight
or in the least air-isolated from the air in the I tube 60 that contains
the optical bench. The need for these isolating windows 86 will depend on
the temperature and pressure levels in the extreme environment, the
chosen probe design and dimensions, and the chamber testing and insertion
zone conditions.
[0050]To prevent any possible damage/breakage to the sensing SiC single
crystal chip (labeled as C 68 in the FIGS. 3-8) due to accidental probe
drop or fast hard moving object striking the tip, an optional protective
tip cage 88 can be designed around a portion of the probe tip 64.
Possible laser drilled holes in the SiC tube cover (ST2 90 in FIG. 4) can
allow the hot gases to easily access the chip 68. FIG. 3 and FIG. 4 shows
various designs using the SiC tube to protect the SiC chip 68. In FIG. 3,
ST5 70e SiC tube is used in two arrangements to protect the SiC chip C
68. Laser bonding can be used to attach the SiC tubes 70a, 70e to each
other or to the SiC chip 68. In either design in FIG. 3, the hot gases
can access the SiC chip 68 directly producing a direct and fast thermal
contact for fast temperature assessment in the
hot placement zone of the
probe 44. In FIG. 4, a closed SiC tube ST2 90 completely protects the SiC
chip C 68. In this case, a physical contact is preferably made between
the SiC chip surface and the inside of the ST2 90 closed tube surface to
make fast heat transfer into the chip. One can also laser drill tiny
holes into the ST2 cover 69 to provide access for the hot gases to the
SiC chip surface. Note the inside surface of the ST2 tube cover 69 is
optically rough so light passing through the SiC chip 68 is not
specularly reflected back to the SMF 74.
[0051]The FIG. 4 probe embodiment uses one long SiC tube SL1 92 to form
the sealed chamber. In addition, it uses one long SiC tube ST2 90 to act
as a protection tube around ST1 92. Also, an adaptor insulator tube I1 94
is used to connect to the optical assembly sitting in another isolated
insulating tube I2 96. Here, two optional glass windows W1 86 and W2 87
are used in the tubes to realize seals and isolate thermal transfer to
optics.
[0052]FIG. 5 shows an alternate design that uses four independent SiC
chips C1, C2, C3, C4, 68a-68d each one mounted in its own SiC tube
assembly 92a-92d as described earlier. In addition, the optical assembly
now has four SMF-FL-M assemblies, each matched to its own SiC chip
target. One large polarizer P 84 is used for all four optical beams. Four
SMFs 74a-74d and related four E 80a-80d cables exit the optical assembly
encased in the insulating tube I2 96. The four FL-M's 76a-76d are mounted
in a holder H 98. Using a 1.times.4 optical switch, any one of the SiC
chip probes can be activated to provide the temperature reading. On the
other hand, all four SMFs 74a-74d can be activated simultaneously for
multiple readings of temperature. Hence, the FIG. 5 probe has built-in
fault-tolerance and a self-calibration feature. In other words, all four
SiC crystals 68a-68d and their related probe sub-assemblies should
provide the same temperature reading, given the temperature is considered
the same and localized due to the small size of the probe tip region. If
the readings from any one or more of the four crystals is different, then
the given probe chip is no-longer calibrated. One can design the probe
using different chip conditions. The baseline design could use four SiC
chips 68a-68d of same thicknesses (and refractive index), and same read
and processing wavelengths. Hence one should expect same temperature
readings for the same normalized optical power data from all four probe
sub-assemblies. This design ensures that the overall 4-channel probe is
calibrated and providing correct temperature readings. One can also
choose SiC chips 68a-68d with different thicknesses and possibly
different refractive indices via different dopant levels in the SiC chips
during fabrication. Also, one can use different wavelengths for
processing for the four different probe sub-assemblies to compute the
actual temperature reading. In short, the FIG. 5 probe design provides
four independent yet simultaneous channels of optical power data that can
be used for multi-dimensional signal processing to produce a robust and
highly accurate temperature measurement. In effect, note that the chip
thicknesses (and refractive indices) and wavelengths used for optical
power data generation can be chosen such that unambiguous temperature
measurements can be made over a designed temperature range using a
particular signal processing formula consisting of a function of the
measured normalized minimal four optical power values. The nature of the
formula is unique to the probe design and measurement ranges. A simple
example formula might be (P1+P3+ P2P4)/(P1+P2+P3+P4+ P1P2). The idea is
that the function value is unique over the design temperature range and
hence the temperature measurement is unambiguous. Of course, the earlier
described two wavelength phase-based signal processing (see N. A. Riza
and F. Perez, "High Temperature Minimally Invasive Optical Sensing
Modules," for which a provisional application was filed on Jul. 23, 2004,
Application No. 60/590,672; a second provisional was filed on Dec. 7,
2004, Application No. 60/633,900; and for which a non-provisional
application for United States patent was filed on Jul. 20, 2005,
application Ser. No. 11/185,540; N. A. Riza, M. A. Arain, and F. Perez,
"Harsh Environments Minimally Invasive Optical Sensing Technique for
Extreme Temperatures: 1000.degree. C. and Approaching 2500.degree. C.,"
in Proceedings of the 17.sup.th Optical Fiber Sensors Conference, (SPIE
2005) Vol. 5855, p. 687; N. A. Riza, M. A. Arain, and F. Perez, "Harsh
Environments Minimally Invasive Optical Sensor using Freespace Targeted
Single Crystal Silicon Carbide," to appear in IEEE Sensors J., accepted
(2005) can also be used with the described probe designs to produce the
unambiguous temperature data.
[0053]FIG. 6 shows an another example probe 44 that has a wireless
implementation allowing temperature sensing of a moving part such as a
rotating element, such as a wheel 114 or a turbine blade. The SiC chip C1
101a is mounted on a short SiC tube ST1 110 using laser bonding. The SiC
tube 110 is mounted using a fitting FT1 112 to the wheel base 104 of the
wheel 114. The probe 44 is disposed proximate to a support structure,
such as by being inserted into a wheel axle rod fitting 108. The probe 44
is based on a SiC tube 100 with an optional exit glass window W1 86. The
optical assembly 63 in the probe 44 is similar to the earlier described
(e.g., FIG. 3) design with an optional glass window W2 87. The laser beam
66 from the probe 44 hits the chip C1 101a every one revolution of the
wheel 114. The probe 44 can use a pulsed high power laser synchronized
with the wheel rotation to enable high efficiency optical data
processing. Note that multiple SiC chips (e.g., C2 101 b and C3 101c) can
be added to the moving part to add redundancy/fault-tolerance to the
measurement system. Also, using multiple SiC chips at different locations
produces a distributed wireless temperature measurement system. Note that
a collinear additional visible laser beam can be used for alignment as
well as keeping the SiC chip clean off debris, etc, by laser burning any
deposits on the chips 101a-101c.
[0054]FIG. 6 shows a SiC single crystal chip 101a mounting where the laser
bonding zone 116 forms at outer ring on the chip 101a. Hence, the chip
101a is in a way clamped to the SiC tube 110 with the internal chip
region 118 free to deform under high temperature high pressure
differential conditions. Given a large diameter (e.g., 5 mm) of the SiC
chip 101a, thermal and pressure effects have minimal local effects in the
inner ring (e.g., <3 mm diameter) of the chip. This inner localized
and flat region of the chip is targeted by the laser beam for proper
temperature readings.
[0055]FIG. 7 shows an alternate mounting of the SiC chip 101a for
moving-parts or stationary but targeted temperature sensing applications.
FIG. 7(a) shows one design using the previously mentioned SiC chip 101a
laser-bonded mounting onto a SiC tube 110. The key point to note here is
that the tube 110 outer diameter is smaller than the SiC chip 101a
diameter, thus allowing the chip boundary to expand as needed due to
temperature effects without deforming the outer part of the chip 101a.
More importantly, under high pressure conditions, the pressure is the
same on both sides of the chip 101a in the region that is the outer
boundary 118 of the chip 101a. Hence, pressure will essentially not
effect the chip flatness at these boundary 118 location. Hence, the
targeted temperature sensing beam must strike the chip at this outer
free-moving boundary 118 zone of the SiC chip 101a. FIG. 7(b) shows an
alternate mounting design where the SiC chip 101a is laser bonded to a
SiC form (e.g., recrystalized or polycrystalline SiC) substrate 120 where
the entire central region 116 of the SiC chip 101a is laser-bonded to the
substrate 120. This design again leaves the boundary 118 of the chip 101a
free for expansion due to thermal effects. Again, pressure or changing
pressure does not effect the SiC chip 101a as the pressure P is the same
on both sides of the SiC chip 101a.
[0056]Previously, numerous works have been conducted to measure pressure.
Pressure sensors have been built by utilizing the variation in the
resistance or capacitance of a device under pressures. Prototype silicon
carbide (SiC) high temperature piezoresistive pressure sensors were
batch-fabricated at the NASA John Glenn Research Center by producing the
diaphragms using a chemical micromachining process, and the sensors
showed promise and were demonstrated to operate up to 500.degree. C. [A.
A. Ned, A. D. Kurtz and R. S. Okojie, High temperature pressure sensors
made from silicon carbide, NASA Tech Briefs, LEW-16772, Glenn Research
Center, Cleveland, Ohio, January 2000]. Okojie et al. [R. S. Okojie, A.
A. Ned and A. D. Kurtz, Operation of .alpha.(6H)--SiC Pressure Sensor at
500.degree. C., 1997 International Conference on Solid-State Sensors and
Actuators, (Institute of Electrical and Electronics Engineers, Inc., New
Jersey, 1997), pp. 1407-1409] fabricated and tested piezoresistive
pressure sensors with full scale output 40.66 and 20.03 mV at 23.degree.
C. and 500.degree. C., respectively, at 1000 psi. Ziermann et al. [R.
Ziermann, J. von Berg, W. Reichert, E. Obermeier, M. Eickhoff and G.
Krotz, A High Temperature Pressure Sensor with .beta.-SiC Piezoresistors
on SOI Substrates, 1997 International Conference on Solid-State Sensors
and Actuators, (Institute of Electrical and Electronics Engineers, Inc.,
New Jersey, 1997), pp. 1411-1414] used Silicon Carbide on Insulator
(SiCOI) to create a piezoresistive pressure sensors and tested its
operation between room temperature and 500.degree. C. They reported the
sensitivity of the device to be 20.2 .mu.V/VkPa at room temperature.
Since these SiC sensors are based on the principle of piezoresistance,
micropipe defects in SiC negatively impact performance. Further research
is necessary to harness the full potentials of SiC as efficient high
temperature pressure sensors surpassing the capability of silicon-based
sensors. Moreover, these SiC MEMS pressure sensors are not wireless
passive devices as described for our optical sensor. In other words,
electronic power and processing is done on chip that is also being
simultaneously exposed to the changing high pressure and temperature
environment. In effect, all the processing in the chip must withstand the
environmental effects.
[0057]Works on producing a wireless pressure sensor includes: A Dehennis,
K. D. Wise, "A double-sided single-chip wireless pressure sensor," 15th
IEEE International Conference on MEMS, 2002; O Akar, T Akin, K Najafi, "A
wireless batch sealed absolute capacitive pressure sensor," Sensors and
Actuators A: Physical, 2001; G Schimetta, F Dollinger, R Weigel, "A
wireless pressure-measurement system using a SAW hybrid sensor," IEEE
Transactions on Microwave Theory and Techniques, 2000. This highlighted
sensors require on-chip power plus electronics and contacts that are
non-robust to high temperatures. Another design described is passive,
that by M A Fonseca, J M English, M von Arx, M G Allen, "Wireless
micromachined ceramic pressure sensor for high-temperature applications,"
Journal of Microelectromechanical Systems, 2002. Nevertheless, this
design presently has limitations in temperature (<400 C) and pressure
(<7 bars) ranges of operations.
[0058]In silicon technology, p-n junction-isolated piezoresistors are used
as pressure sensors for temperatures less than 175.degree. C., and
silicon-on-insulator (SOI) sensors for temperatures up to 500.degree. C.
Other techniques have also been investigated to measure pressure. Leading
fiber-optic sensors such as using fiber Fabry-Perot interference or
in-fiber Bragg Gratings with wavelength-based processing by use of the
fiber wire for light delivery and light return do not form the needed
wireless pressure sensor (see C. E. Lee and H. F. Taylor, "Sensors for
smart structures based on the Fabry-Perot interferometer," Chapter 9, pp.
249-270, Fiber Optic Smart Structures, Ed. Eric Udd, Wiley, 1995; R.
Duncan, D. Gifford, V. Rajendran, "OFDR tracks temperatures on power
generators," Laser Focus World Magazine, p. 89, October 2003; A. D.
Kersey, et.al., "Fiber Grating Sensors," IEEE/OSA J. Lightwave Tech.,
Vol. 15, No. 8, pp. 1442-1463, August 1997; Brian Culshaw, "Optical Fiber
Sensor Technologies: Opportunities and Perhaps Pitfalls," IEEE/OSA
Journal of Lightwave Technology, Vol. 22, No. 1, pp 39-50, January 2004).
Optically reflective [L. Tenerz, L. Smith and B. Hok, A Fiber Optic
Silicon Pressure Microsensor for measurements in Coronary Arteries, in
Proc. Sixth Int. Conf. Solid State Sensors and Actuators, Transducers
'91, San Francisco, 1991, pp. 1021-1023] and interferometric [T.
Katsumata, Y. Haga, K. Minami and E. Esashi, Micromachined 125 .mu.m
Diameter Ultra-Miniature Fiber-Optic Pressure Sensor for Catheter, Trans.
Inst. Electr. Eng. Jpn. Part E, Vol. 120E, 2000, pp. 58-63; J. Zhou, S.
Dasgupta, H. Kobayashi, J. M. Wolff, H. E. Jackson and J. T. Boyd,
Optically interrogated MEMS pressure sensors for propulsion applications,
Opt. Eng., Vol. 40, 2001, pp. 598-604; D. C. Abeysinghe, S. Dasgupta, J.
T. Boyd and H. E. Jackson, A novel MEMS pressure sensor fabricated on an
optical fiber, IEEE Photonics Tech. Letts., Vol. 13, 2001, pp. 993-995]
techniques have also been investigated. The interferometric techniques
were based on Fabry-Perot interferometer/cavity formed by etching a glass
substrate or the tip of an optical fiber and enclosing the etched volume
with a silicon diaphragm. The materials in these optical devices were
glass and silicon which will melt at the high temperature environment in
NASA planetary applications. Recently further work in optical pressure
sensor has been reported as stated next, but all have their limitations
due to the exposure of their non-robust sensing element in the extreme
NASA environment. These are: W. Li, D. C. Abeysinghe, J. T. Boyd,
"Wavelength Multiplexing of microelectromechanical system pressure and
temperature sensors using fiber Bragg gratings and arrayed waveguide
gratings," Optical Engg., Vol. 42, 2, pp. 431-438, February 2003; W. Li,
D. C. Abeysinghe, J. T. Boyd, "Multiplexed sensor system for simultaneous
measurement of pressure and temperature," Optical Engineering., Vol. 43,
1, pp. 148-156, January 2004; D Guo, W. Wang, R Lin, "Theoretical
analysis and measurement of the temperature dependence of a micromachined
Fabry-Perot pressure sensor," Applied Optics, Vol. 44, 2, pp. 249-256,
Jan. 10, 2005; Y. Zhu, A. Wang, "Miniature fiber-optic pressure sensor,"
IEEE P
hoton. Tech. Lett., Vol. 17, 2, pp. 447-449, February 2005; J. Xu,
G. Pickrell, X. Wang, W. Peng, K. Cooper, A. Wang, "A novel temperature
insensitive optical fiber pressure sensor for harsh environments," IEEE
Photon. Tech. Lett., Vol. 17, 4, pp. 870-872, April 2005; D. Donlagic and
E. Cibula, "All-fiber high sensitivity pressure sensor with SiO2
diaphragm," Optics Letters, Vol. 30, No. 16, pp. 2071-2073, Aug. 15,
2005. All these fiber-based optical pressure sensors are non-wireless
design.
[0059]FIG. 8 shows another example probe 44 that can simultaneously
measure temperature and pressure. Temperature is measured using the
previously described probe designs (FIGS. 1-7) where the localized
central flat portion of the SiC chip 68 is targeted and read by the laser
beam 66 to estimate the chip temperature. In the FIG. 8 design, the same
principle is implemented except that a two dimensional (2-D) large area
optical detector such as a CCD camera is used to measure the optical
power. In this embodiment, a large diameter beam 67 (e.g., 10 mm) is
created by beam expansion optics (lenses S1 127 and S2 126) in the
optical assembly such that this large beam 67 strikes nearly the entire,
or a majority of, surface area of the used large diameter SiC chip 68.
The chip 68 is laser bonded to a large diameter SiC tube ST1 70a that is
vacuum sealed at the other end using a glass window W1 86. When external
pressure P is applied to the outer surface 69 of the SiC 68 in the probe
44, the chip 68 deforms in-words. Recall that the SiC chip 68 acts like a
Fabry-Perot cavity. When the pressure deforms the two surfaces of the
chip cavity, like with spherical surfaces as shown in FIG. 8, the optical
interference provided by the chip 68 is not uniform over the chip surface
71. Hence the received beam directed to the 2-D camera 122 by the beam
splitter 124 shows a given optical interference pattern for a given
pressure P and temperature T condition. Note that the SiC front 71 and
back 69 surfaces will have unique deformations due to the external
pressure effect. Hence the optical reflections caused by these two
independent surfaces will have pressure and temperature dependent unique
reflected wavefronts that will interfere together at the CCD plane to
produce a unique pressure and temperature dependent 2-D interferogram. By
processing the central zone of the beam on the chip (and hence the
central zone of the detected interferogram), one can compute the
temperature of the chip. This is like the FIG. 1-7 temperature probe
designs. Hence, knowing the effect of temperature on the chip without
pressure effects, one can deduce how much of the global interference
pattern was produced due only to pressure P. Using advanced image
processing, such as in temperature and pressure processor 128, methods on
the measured interferogram and previously measured temperature only and
pressure only probe calibration data, one can compute the measured
temperature and pressure from the probe design in FIG. 8. The key point
to note is that temperature is a spatially local effect on the SiC chip
68 while pressure is mostly a spatially distributed or global effect on
the SiC chip 68. Using a small chip diameter can help reduce pressure
effects on the chip and hence make it ideal for a temperature-only probe,
while using large chip diameters will enhance pressure effects on the SiC
single crystal chip 68 allowing both pressure and temperature
measurements. Note that since the SiC chip 68 is 2-D and the
interferogram is 2-D, one could deduce pressure and gas flow
directions/distributions on the SiC chip zone by using image processing
methods.
[0060]A remote pressure sensor is needed in many applications. Described
is Silicon Carbide (SiC) weak lensing effect based wireless optical
sensors that allows safe, repeatable, and accurate pressure measurement
suitable for harsh environments. This completely passive front-end sensor
design uses a remoted free-space optical beam that targets a single
crystal SiC chip fitted as an optical window within a pressure capsule.
With increasing differential capsule pressure, the SiC chip forms a weak
convex mirror with a changing focal length. By monitoring the chip
reflected unique light beam fringe pattern magnification, pressure in the
capsule is determined. SiC is chosen as the front-end all-passive sensor
material due to its robust mechanical, chemical, and optical properties
when subject to extreme environments with respect to temperature,
pressure and chemically corrosive conditions.
[0061]FIG. 9 shows an example pressure sensor 130 using high pressure
capsule (HPC). A collimated laser beam 67 passes through a Beam Splitter
(BS) 124 and after traveling a distance d.sub.1 targets the SiC chip 68
fitted as a window in an aperture 133 in a wall 135 of the High Pressure
Capsule (HPC) 132. The beam reflections from the SiC chip 68 travel a
distance of d.sub.1+d.sub.2 and are captured by an Optical Image Detector
(OID) 122. Because laser beams can be highly collimated and the pressure
effect on the SiC chip 68 is a mechanical deformation resulting in a weak
lensing effect, the distance d.sub.1 can be designed to be rather large,
e.g. several meters. Thus, only the SiC-based HPC 132 is placed in the
hostile zone while the transceiver module containing the laser source 36,
alignment optics, and the OID 122 is meters away, allowing safe and
remote pressure measurement. Note that the beam reflections from the SiC
chip 68 are produced as reflections from the chip front 71 and back 69
surfaces, giving an interferometric fringe pattern that is observed by
the OID 122. These fringes contain information about the relative phase
differences between the two SiC surfaces 69,71, and are unique for a
given SiC chip 68. In the absence of any differential pressure, i.e.,
pressure inside the capsule 132 is equal to the ambient atmospheric
pressure outside the capsule 132, the SiC chip 68 acts like a flat
mirror. Thus the laser beam 66 after reflection from the chip 68
continues to diverge in accordance with Gaussian beam propagation and
divergence. However, in the presence of differential pressure P, the SiC
chip with a circular pressure boundary of radius "a" (in cm) bulges
outwards with a maximum central displacement of w.sub.max (in cm) given
by:
w max ( P ) = Pa 4 64 D , and ( 1 A )
w max ( P ) = Pa 4 64 D ( 5 + v 1 + v )
( 2 A )
for the Clamped-Edge model (Eqn. 1A) and Supported-Edge model (Eqn. 2A),
respectively. Here, D is the SiC rigidity constant and v is its Poisson's
ratio. The SiC chip 68 under differential pressure P acts as a weak
convex mirror or equivalently as a concave lens with focal length f(P) in
cm given by:
f ( P ) = w max 2 ( P ) + a 2 4 w max
( P ) .times. 10 4 cm . ( 3 A )
[0062]FIG. 10 shows the weak lens optical ray-trace model 134 used to
design the described remote pressure sensor where the SiC chip 68 acts
like a pressure dependant concave lens 136 that diverges the input laser
beam 66. Thus the beam diameter D(P) measured by the OID provides a value
for the sensed pressure P. For example, at P=0, f=.infin. and
D(P)=D.sub.0, the initial beam diameter on the OID. Given that the
illuminated SiC chip naturally produces a specific fringe pattern via its
Fabry-Perot etalon behavior, a given chip that produces a linear fringe
pattern due to its slight wedge nature can be used under certain
circumstances to design the pressure sensor. In this case, one can
essentially use the OID measured fringe period to determine the pressure
P. Moreover, using FIG. 10, one can define a pressure dependent sensor
magnification factor M given by:
M ( P ) = D ( P ) D 0 = 1 + ( d 1 + d 2 )
f ( P ) , ( 4 A )
with d.sub.1+d.sub.2 in cm and where X(P) is the fringe period for
pressure P and X.sub.0 is the fringe period for P=0. Thus, by measuring M
using the OID, one can remotely deduce the pressure P using the
calibration data stored in the Computer Image Processor (CIP). For sensor
calibration, one uses a reference pressure gauge to record P versus M
data as P is varied over a desired calibration range. With an increasing
temperature of the SiC chip 68, one expects an increase in chip thickness
via thermal expansion and an increase in material refractive index. Both
these factors uniformly change the optical path lengths for the
interfering beams from the SiC chip surfaces 69, 71, thus causing fringe
pattern shifts with temperature. Nevertheless, the SiC chip weak lens
effect that controls beam magnification is expected to be dominated by
the pressure-based chip deformation, making the described pressure sensor
essentially temperature independent when deploying CTE matched packaging
for the SiC chip. Note that one can tune the laser wavelength to optimize
received optical power so the receive optical beam boundary at the OID
can be clearly measured to access receive beam magnification change due
to pressure effects.
[0063]Single crystal 6H--SiC is a highly desirable front-end sensor
material as its melting temperature is around 2500.degree. C. Moreover,
apart from its resistance to chemical attack and excellent optical
properties, thick (e.g., 300 .mu.m) single crystal 6H--SiC also has
powerful mechanical properties via its elastic, shear, and bulk modulus
values and Poisson ratio. Therefore, the SiC chip forms a robust extreme
environment front-end sensor for laser beam-based wireless access.
Nevertheless, fiber-optics can play an important role in the described
hybrid sensors by providing a wired light delivery mechanism to the
wireless port position in the sensor system. Well protected custom Single
Mode Fibers (SMFs) made of silica can operate near temperatures reaching
1000.degree. C., thus forming an excellent wired non-line of sight
delivery mechanism to a location near the extreme environment where
temperatures are still reasonable compared to the extreme environment
temperature (e.g., 1500.degree. C. in a combustion chamber).
[0064]FIG. 11(a,b) shows some example designs on how SMFs can be combined
with the described SiC chip-based sensing principles to realize compact
versions of the remoted hybrid sensors. In essence, the distance between
the SiC chip and the launch SMF point is small, forming an all-in-one
compact fiber remoted sensing head, much like traditional SMF sensors.
FIG. 11(a) shows a temperature sensor embodiment 138 that is based on
localized or point targeting of the SiC chip 68 to measure temperature
dependent optical path length change (OPL). By making the light read zone
140 on the chip 68 small compared to the chip size 142, one can
essentially remove the effects of pressure on the chip localized OPL.
Such targeting is achieved using a point-to-point imaging lens 144
formation between the SMF-free-space interface 148 and the SiC chip C 68.
Because the described chip thickness is small (e.g., 300 .mu.m) versus
the imaging lens focal length (e.g., 3 cm) deployed, the chip front 71
and back 69 faces retro-reflect the sensing light back to the SMF 74 for
sensor signal processing. Each SMF 74 can have an optional electronically
controlled tilt control stage to keep the SMF 74 aligned with the SiC
chip 68. The entire assembly can be mounted in an appropriate ceramic
package. To enable a pressure sensor 150, a collimating optical beam
architecture shown in FIG. 11(b) is used where a majority of chip C 68 is
illuminated. The distance between the collimating lens and the SiC chip
68 can be designed to be as large or small as needed for the remoting
application. As relative pressure between the chip sides builds, the chip
68 deforms and acts like a convex mirror, reducing the optical coupling
between the SMF 74 and the chip 68. Hence, a pressure change causes
wavefront optical beam spoiling. As SMFs are very sensitive to wavefront
quality, one sees a different coupling efficiency. Thus by monitoring the
SMF coupling efficiency, pressure can be estimated assuming the chip
packaging is designed such that temperature variations cause minimal chip
deformation effects. In case temperature effects should not be ignored,
both temperature plus pressure may need to be measured to generate a
calibration table for optical coupling efficiency.
[0065]The key to pressure sensing using SiC involves global targeting of
the SiC chip with received light pattern undergoing image (versus point
zone) processing. FIG. 12 shows such a design using a long remoting probe
44. Here, note the large beam cross-section of the targeting beam that
strikes the SiC acting as a weak convex mirror under applied pressure.
This weak lensing changes the detected size of the optical beam image at
the receiver optics that can be an optical multi-fiber bundle 154 or a
miniature camera 122 as in FIG. 8. Using image processing, a pressure
versus image size chart can be generated for sensor calibration and
pressure measurement.
[0066]The more powerful sensor is one that can simultaneously provide both
temperature and pressure data as in FIG. 8. FIG. 13 shows an alternate
implementation of the described hybrid sensor concept that uses a
remotely placed all-passive optical sensor capsule 152 made of single
crystal SiC chip 68 acting as the capsule window and a pressure sealed
capsule assembly 154 made of a suitable high pressure high temperature
material such as the previously mentioned sintered SiC tube. The FIG. 13
design is suited for near access sensing within the hot gas environment
of a power plant. The capsule 152 has a high pressure connector 156 that
interfaces to the high pressure hot gas flow system that is linked to the
high temperature high pressure hot gas flow 158 such as a fossil fuel
plant under test. The SiC optical window sits in a specially designed
sealed pressure seat that creates the desired high pressure boundary
conditions for the deployed SiC chip 68 within the capsule 152. One can
also envision the FIG. 13 pressure sensor module used as a pressure stick
inserted into a pressure sealed cavity to allow deep access pressure
readings such as well within a combustion chamber. Hence, depending on
the application, appropriate packaging must be deployed.
[0067]In FIG. 13, the reflected beam enters a light path containing a
pin-hole (PH1) 160 that accepts only the on-axis rays from the SiC chip
68. After the pin-hole 160, a point detector D1 162 picks up the optical
power from the selected on-axis rays. Thus, the localized effect is
captured by monitoring the on-axis central rays from the SiC chip 68. As
the temperature changes, the SiC chip optical path length (OPL) changes
dominated by the material refractive index change. By measuring this OPL
change, the temperature of the chip 68 can be measured. On the
other-hand, the sensing straight beam passes through PBS2 164 to impinge
on a two dimensional (2-D) optical detector D2 122 such as a CCD chip. As
pressure changes inside the capsule (outside the capsule is 1 atm), the
SiC chip 68 deforms to produce a convex mirror effect. Note that only
near the on-axis condition are the faces of the chip normal to the
incident beam, hence producing true retro-reflection to create beams that
pass via the pinhole 160 to D1 162 to make the temperature-only
measurement. In effect, as pressure (P) changes, the on-axis ray bundle
remains essentially the same allowing a pressure independent temperature
measurement. It is important to note that the SiC chip 68 and chip
seating in the capsule 152 can be designed such that the out-of-plane
deflection is mainly caused by internal pressure change with minimal
contribution from temperature (T) effects. Such a design is possible by
essentially using a chip packaging/boundary material with a similar CTE
to single crystal SiC 68 like the sintered SiC tube material where CTE's
match. Pressure (P) plus temperature data is picked up by the optical
detector 122 and then processed to determine true pressure readings.
* * * * *